Information card for entry 7159962
Formula |
C H N O P |
Calculated formula |
C3.2 H3.2 N0.2 O0.6 P0.2 |
Title of publication |
Efficient synthesis of α-amino-vinylphosphine oxides from alkyl nitriles via manganese-catalyzed phosphinoenamination |
Authors of publication |
Guo, Sheng Mei; Ding, Anjun; Junpeng, Yang; Liu, Xiaoyong; Sun, Runbo; Zhang, Zheng; Luo, Ruihang; Tang, Wentao; Cai, Hu; Fu, Zhengjiang; Liu, Xingyu |
Journal of publication |
Organic & Biomolecular Chemistry |
Year of publication |
2024 |
a |
22.033 ± 0.002 Å |
b |
13.718 ± 0.002 Å |
c |
10.1323 ± 0.0012 Å |
α |
90° |
β |
97.804 ± 0.003° |
γ |
90° |
Cell volume |
3034.1 ± 0.6 Å3 |
Cell temperature |
296 ± 2 K |
Ambient diffraction temperature |
296.15 K |
Number of distinct elements |
5 |
Space group number |
15 |
Hermann-Mauguin space group symbol |
C 1 2/c 1 |
Hall space group symbol |
-C 2yc |
Residual factor for all reflections |
0.1135 |
Residual factor for significantly intense reflections |
0.0881 |
Weighted residual factors for significantly intense reflections |
0.2345 |
Weighted residual factors for all reflections included in the refinement |
0.2628 |
Goodness-of-fit parameter for all reflections included in the refinement |
1.037 |
Diffraction radiation wavelength |
0.71073 Å |
Diffraction radiation type |
MoKα |
Has coordinates |
Yes |
Has disorder |
No |
Has Fobs |
No |
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https://www.crystallography.net/7159962.html