Information card for entry 7160140

Structure parameters

• Formula: C26 H37 N3 O2 S Si
• Calculated formula: C26 H37 N3 O2 S Si
• Title of publication: Facile access to α-silylmethylamidines by BF3-catalyzed hydroamination of silylynamides with amines
• Authors of publication: Lu, Fei; Li, Zengzeng; Wang, Yulu; Liu, Guoliang; Niu, Guangguo; Wang, Guanghui; Zhao, Ximei
• Journal of publication: Organic & Biomolecular Chemistry
• Year of publication: 2024
• a: 19.9676 ± 0.0006 Å
• b: 7.9854 ± 0.0002 Å
• c: 16.986 ± 0.0006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2708.41 ± 0.14 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.0663
• Residual factor for significantly intense reflections: 0.0477
• Weighted residual factors for significantly intense reflections: 0.1196
• Weighted residual factors for all reflections included in the refinement: 0.1408
• Goodness-of-fit parameter for all reflections included in the refinement: 1.066
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No