Co-crystallization of a versatile building block 4-amino- 3,5-bis(4-pyridyl)-1,2,4-triazole with R-isophthalic acids (R = ‒H, ‒NH2, ‒SO3H, and ‒COOH): polymorphism and substituent effect on structural diversity
Authors of publication
Du, Miao; Jiang, Xiu-Juan; Tan, Xue; Zhang, Zhi-Hui; Cai, Hua
Journal of publication
CrystEngComm
Year of publication
2009
Journal volume
11
Journal issue
3
Pages of publication
454
a
6.255 ± 0.002 Å
b
7.187 ± 0.002 Å
c
20.272 ± 0.004 Å
α
83.78 ± 0.03°
β
86.62 ± 0.03°
γ
79.03 ± 0.02°
Cell volume
888.7 ± 0.4 Å3
Cell temperature
294 ± 2 K
Ambient diffraction temperature
294 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1681
Residual factor for significantly intense reflections
0.0503
Weighted residual factors for significantly intense reflections
0.0853
Weighted residual factors for all reflections included in the refinement
0.1037
Goodness-of-fit parameter for all reflections included in the refinement
