Information card for entry 7200319

Structure parameters

• Formula: Co10 H176 K15 Li5 O272 P8 W48
• Calculated formula: Co8.4 K14.6 Li5 O264.2 P8 W48
• Title of publication: Controlling nucleation of the cyclic heteropolyanion {P8W48}: a cobalt-substituted phosphotungstate chain and network
• Authors of publication: Mitchell, Scott G.; Gabb, David; Ritchie, Chris; Hazel, Nick; Long, De-Liang; Cronin, Leroy
• Journal of publication: CrystEngComm
• Year of publication: 2009
• Journal volume: 11
• Journal issue: 1
• Pages of publication: 36
• a: 15.8572 ± 0.0006 Å
• b: 20.4459 ± 0.0008 Å
• c: 23.548 ± 0.0009 Å
• α: 106.003 ± 0.002°
• β: 103.677 ± 0.002°
• γ: 95.378 ± 0.002°
• Cell volume: 7026.7 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1324
• Residual factor for significantly intense reflections: 0.0573
• Weighted residual factors for significantly intense reflections: 0.1216
• Weighted residual factors for all reflections included in the refinement: 0.1536
• Goodness-of-fit parameter for all reflections included in the refinement: 1.008
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No