Information card for entry 7200733

Structure parameters

• Formula: Bi2 H62 Na5 O107 Pd4.5 W22
• Calculated formula: Bi2 Na1.7 O104.6 Pd4.5 W22
• Title of publication: The palladium(II)-decorated 22-tungsto-2-bismuthate(III), [Pd3(H2O)9Bi2W22O76]8−
• Authors of publication: Bi, Li-Hua; Dickman, Michael H.; Kortz, Ulrich
• Journal of publication: CrystEngComm
• Year of publication: 2009
• Journal volume: 11
• Journal issue: 6
• Pages of publication: 965
• a: 12.8207 ± 0.0012 Å
• b: 13.1305 ± 0.0014 Å
• c: 17.407 ± 0.002 Å
• α: 108.61 ± 0.007°
• β: 98.928 ± 0.007°
• γ: 109.55 ± 0.006°
• Cell volume: 2501.9 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0817
• Residual factor for significantly intense reflections: 0.0491
• Weighted residual factors for significantly intense reflections: 0.1216
• Weighted residual factors for all reflections included in the refinement: 0.1409
• Goodness-of-fit parameter for all reflections included in the refinement: 1.071
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No