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Information card for entry 7202426
Preview
Coordinates | 7202426.cif |
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Original paper (by DOI) | HTML |
Common name | [{(dmba)Pd}2(m-OAc)(m-N=CPh2)].1(n-hexane) |
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Chemical name | [μ-Acetato-μ-benzophenone iminato- bis{N,N-dimethylbenzylamine-κN,κC-palladium(II)}] 1(n-hexane) |
Formula | C39 H51 N3 O2 Pd2 |
Calculated formula | C39 H51 N3 O2 Pd2 |
Title of publication | Structure‒solid-state CPMAS 13C NMR correlation in palladacycle solvates (pseudo-polymorphs) with a transformation from Z′ = 1 to Z′ = 2 |
Authors of publication | Ruiz, José; Rodríguez, Venancio; Cutillas, Natalia; Hoffmann, Anke; Chamayou, Anne-Christine; Kazmierczak, Karolina; Janiak, Christoph |
Journal of publication | CrystEngComm |
Year of publication | 2008 |
Journal volume | 10 |
Journal issue | 12 |
Pages of publication | 1928 |
a | 14.2859 ± 0.0006 Å |
b | 28.3485 ± 0.0012 Å |
c | 9.2862 ± 0.0004 Å |
α | 90° |
β | 103.894 ± 0.001° |
γ | 90° |
Cell volume | 3650.7 ± 0.3 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 5 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0312 |
Residual factor for significantly intense reflections | 0.0296 |
Weighted residual factors for significantly intense reflections | 0.0717 |
Weighted residual factors for all reflections included in the refinement | 0.0725 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.135 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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