Information card for entry 7203673

Structure parameters

• Formula: C25 H44 N12 Nd2 O17 W
• Calculated formula: C25 H42 N12 Nd2 O17 W
• Title of publication: Three-dimensional Ln<small>^III</small>‒W<small>^IV</small> complexes with cyanido and carboxylato bridges
• Authors of publication: Stefania Tanase; Ferry Prins; Jan M. M. Smits; René de Gelder
• Journal of publication: CrystEngComm
• Year of publication: 2006
• Journal volume: 8
• Journal issue: 12
• Pages of publication: 863
• a: 10.9221 ± 0.0005 Å
• b: 19.266 ± 0.002 Å
• c: 19.4537 ± 0.0009 Å
• α: 90°
• β: 98.385 ± 0.005°
• γ: 90°
• Cell volume: 4049.8 ± 0.5 ų
• Cell temperature: 208 ± 2 K
• Ambient diffraction temperature: 208 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0345
• Residual factor for significantly intense reflections: 0.0254
• Weighted residual factors for all reflections: 0.0585
• Weighted residual factors for significantly intense reflections: 0.0555
• Weighted residual factors for all reflections included in the refinement: 0.0585
• Goodness-of-fit parameter for all reflections: 1.131
• Goodness-of-fit parameter for all reflections included in the refinement: 1.131
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No