Information card for entry 7204134

Structure parameters

• Formula: C36 H40 O6
• Calculated formula: C34 H38 O6
• Title of publication: Serial synthesis of oxa[3.n]cyclophanes and homooxacalix[n]arenes via reductive coupling of arenedialdehydes, and their X-ray structures
• Authors of publication: Komatsu, Naoki; Chishiro, Takefumi
• Journal of publication: Journal of the Chemical Society, Perkin Transactions 1
• Year of publication: 2001
• Journal issue: 13
• Pages of publication: 1532 - 1537
• a: 23.388 ± 0.002 Å
• b: 17.227 ± 0.002 Å
• c: 7.655 ± 0.001 Å
• α: 89°
• β: 89°
• γ: 90°
• Cell volume: 3083.3 ± 0.6 ų
• Cell temperature: 298.2 K
• Ambient diffraction temperature: 298.2 K
• Number of distinct elements: 3
• Space group number: 36
• Hermann-Mauguin space group symbol: C m c 21
• Hall space group symbol: C 2c -2
• Residual factor for significantly intense reflections: 0.0573
• Weighted residual factors for significantly intense reflections: 0.0846
• Goodness-of-fit parameter for significantly intense reflections: 1.398
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No