Information card for entry 7204312

Structure parameters

• Formula: K1.33 O32 P4 W8
• Calculated formula: K1.30688 O32 P4 W8
• Title of publication: Crystal structure of monophosphate tungsten bronze K1.33P4W8O32 at 110 K
• Authors of publication: Dusek, Michal; Lüdecke, Jens; van Smaalen, Sander
• Journal of publication: Journal of Materials Chemistry
• Year of publication: 2002
• Journal volume: 12
• Journal issue: 5
• Pages of publication: 1408
• a: 13.373 ± 0.007 Å
• b: 5.3282 ± 0.0011 Å
• c: 8.926 ± 0.004 Å
• α: 90 ± 0.02°
• β: 100.65 ± 0.04°
• γ: 90 ± 0.02°
• Cell volume: 625.1 ± 0.5 ų
• Cell temperature: 110 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0507
• Residual factor for significantly intense reflections: 0.0283
• Weighted residual factors for significantly intense reflections: 0.053
• Weighted residual factors for all reflections included in the refinement: 0.0597
• Goodness-of-fit parameter for significantly intense reflections: 2.48
• Goodness-of-fit parameter for all reflections included in the refinement: 2.19
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.59 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No