Synthesis of 2-aryl-2H,4H-imidazo[4,5-d][1,2,3]triazoles from triethyl N-(1-ethyl-2-methyl-4-nitro-1H-imidazol-5-yl)phosphorimidate by reaction with aryl isocyanates
Authors of publication
Taher, Abutariq; Eichenseher, Sandra; Slawin, Alexandra M. Z.; Tennant, George; Weaver, George W.
Journal of publication
Journal of the Chemical Society, Perkin Transactions 1
Year of publication
2002
Journal issue
17
Pages of publication
1968
a
7.188 ± 0.002 Å
b
9.088 ± 0.002 Å
c
10.682 ± 0.002 Å
α
88.99 ± 0.02°
β
100.84 ± 0.02°
γ
91.56 ± 0.01°
Cell volume
685 ± 0.3 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0739
Residual factor for significantly intense reflections
0.0517
Weighted residual factors for significantly intense reflections
0.1489
Weighted residual factors for all reflections included in the refinement
0.1656
Goodness-of-fit parameter for all reflections included in the refinement
