Information card for entry 7204628

Structure parameters

• Formula: C48 H43 Cl2 Fe N12 Ni2 O20.5
• Calculated formula: C48 H36 Cl2 Fe N12 Ni2 O20.5
• Title of publication: Controlling the construction of trinuclear, 1-D, and 2-D Ni(ii)Fe(ii)/Fe(ii)Fe(ii) complexes: selective syntheses, structures, and magnetic properties
• Authors of publication: Kamiyama, Asako; Noguchi, Tomoko; Kajiwara, Takashi; Ito, Tasuku
• Journal of publication: CrystEngComm
• Year of publication: 2003
• Journal volume: 5
• Journal issue: 40
• Pages of publication: 231
• a: 8.9267 ± 0.0006 Å
• b: 12.2683 ± 0.0008 Å
• c: 13.3292 ± 0.0009 Å
• α: 90.215 ± 0.002°
• β: 101.813 ± 0.002°
• γ: 97.288 ± 0.002°
• Cell volume: 1416.63 ± 0.16 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1241
• Residual factor for significantly intense reflections: 0.0616
• Weighted residual factors for significantly intense reflections: 0.1428
• Weighted residual factors for all reflections included in the refinement: 0.1688
• Goodness-of-fit parameter for all reflections included in the refinement: 1
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No