Information card for entry 7204811

Structure parameters

• Chemical name: [Pb(dimb)(dmf)(NO3)2]
• Formula: C18 H23 N7 O7 Pb
• Calculated formula: C18 H23 N7 O7 Pb
• Title of publication: Novel Pb(ii) coordination frameworks: synthesis, crystal structures and unusual third-order nonlinear optical propertiesElectronic supplementary information (ESI) available: crystal packing diagram of complex 2. See http://www.rsc.org/suppdata/jm/b3/b315682f/
• Authors of publication: Sui, Bin; Zhao, Wei; Ma, Guohong; Okamura, Taka-aki; Fan, Jian; Li, Yi-Zhi; Tang, Sing-Hai; Sun, Wei-Yin; Ueyama, Norikazu
• Journal of publication: Journal of Materials Chemistry
• Year of publication: 2004
• Journal volume: 14
• Journal issue: 10
• Pages of publication: 1631
• a: 11.248 ± 0.011 Å
• b: 13.72 ± 0.03 Å
• c: 17.3 ± 0.02 Å
• α: 71.56 ± 0.15°
• β: 83.08 ± 0.11°
• γ: 68.62 ± 0.15°
• Cell volume: 2358 ± 7 ų
• Cell temperature: 200 K
• Ambient diffraction temperature: 200 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0703
• Residual factor for significantly intense reflections: 0.0397
• Weighted residual factors for significantly intense reflections: 0.0785
• Weighted residual factors for all reflections included in the refinement: 0.084
• Goodness-of-fit parameter for all reflections included in the refinement: 0.866
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No