Information card for entry 7205538

Structure parameters

• Formula: C8 H5 Cu K4 N O84 P2 Rb4 Sn W19
• Calculated formula: C8 H5 Cu K4 N O84 P2 Rb4 Sn W19
• Title of publication: Controlled synthesis of a functionalized polytungstate ligand and a {MaMbMc(PW9)2} sandwich complex
• Authors of publication: Cao, Rui; O'Halloran, Kevin P.; Hillesheim, Daniel A.; Lense, Sheri; Hardcastle, Kenneth I.; Hill, Craig L.
• Journal of publication: CrystEngComm
• Year of publication: 2011
• Journal volume: 13
• Journal issue: 3
• Pages of publication: 738
• a: 12.071 ± 0.007 Å
• b: 17.845 ± 0.01 Å
• c: 24.577 ± 0.013 Å
• α: 69.222 ± 0.007°
• β: 80.827 ± 0.008°
• γ: 70.812 ± 0.008°
• Cell volume: 4669 ± 5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 10
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0596
• Residual factor for significantly intense reflections: 0.0432
• Weighted residual factors for significantly intense reflections: 0.1081
• Weighted residual factors for all reflections included in the refinement: 0.1155
• Goodness-of-fit parameter for all reflections included in the refinement: 1.034
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No