Information card for entry 7207671

Structure parameters

• Formula: C104 H87 Co8 N9 O18
• Calculated formula: C104 H87 Co8 N9 O18
• Title of publication: Old dog, new tricks: 2,2′-biphenol as a bridging and book-end ligand in discrete and extended Co(ii) architectures
• Authors of publication: Berg, Nelly; Taylor, Stephanie M.; Prescimone, Alessandro; Brechin, Euan. K.; Jones, Leigh F.
• Journal of publication: CrystEngComm
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 8
• Pages of publication: 2732
• a: 12.7876 ± 0.0005 Å
• b: 19.4297 ± 0.0007 Å
• c: 20.1892 ± 0.0008 Å
• α: 90°
• β: 103.649 ± 0.004°
• γ: 90°
• Cell volume: 4874.5 ± 0.3 ų
• Cell temperature: 149.9 K
• Ambient diffraction temperature: 149.9 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1285
• Residual factor for significantly intense reflections: 0.0698
• Weighted residual factors for all reflections: 0.0331
• Weighted residual factors for significantly intense reflections: 0.0232
• Weighted residual factors for all reflections included in the refinement: 0.0232
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1163
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No