Information card for entry 7207825

Structure parameters

• Formula: C28 H24 N6 Ni O2 S2
• Calculated formula: C28 H24 N6 Ni O2 S2
• Title of publication: Three routes to nickel(ii) salicylaldehyde 4-phenyl and 4-methylthiosemicarbazonato complexes: mechanochemical, electrochemical and conventional approach
• Authors of publication: Cindrić, Marina; Uzelac, Marina; Cinčić, Dominik; Halasz, Ivan; Pavlović, Gordana; Hrenar, Tomica; Ćurić, Manda; Kovačević, Davor
• Journal of publication: CrystEngComm
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 9
• Pages of publication: 3039
• a: 11.8765 ± 0.00054 Å
• b: 22.5378 ± 0.0012 Å
• c: 10.78016 ± 0.00051 Å
• α: 90°
• β: 116.174 ± 0.0029°
• γ: 90°
• Cell volume: 2589.6 ± 0.2 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• RFsqd: 0.0162
• Method of determination: powder diffraction
• Diffraction radiation wavelength: 1.54059 Å
• Diffraction radiation type: CuKα_1
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No