Information card for entry 7207866

Structure parameters

• Formula: C12 H40 Ge2 N8 S6
• Calculated formula: C12 H40 Ge2 N8 S6
• SMILES: C(CN(CC[NH3+])CC[NH3+])N.[S-][Ge]1(S[Ge]([S-])(S1)[S-])[S-].C(CN(CC[NH3+])CC[NH3+])N
• Title of publication: Solvothermal synthesis, crystal structures and properties of three new thiogermanates: the only example of the thiogermanate anion [Ge2S6]4− as a bridging ligand to a lanthanide complex ion
• Authors of publication: Liu, Xing; Hu, Feilong; Zhou, Jian; An, Litao; Liang, Dawen; Lin, Jianwu
• Journal of publication: CrystEngComm
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 10
• Pages of publication: 3464
• a: 25.264 ± 0.009 Å
• b: 7.313 ± 0.003 Å
• c: 16.584 ± 0.006 Å
• α: 90°
• β: 122.616 ± 0.004°
• γ: 90°
• Cell volume: 2580.8 ± 1.7 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0438
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for significantly intense reflections: 0.0943
• Weighted residual factors for all reflections included in the refinement: 0.1035
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No