Information card for entry 7208330

Structure parameters

• Common name: hexakis(N-methylimidazole)nickel(II) bistriflimide
• Chemical name: hexakis(N-methylimidazole)nickel(II) bis(trifluoromethyl)sulfonylimide
• Formula: C28 H36 F12 N14 Ni O8 S4
• Calculated formula: C28 H36 F12 N14 Ni O8 S4
• Title of publication: Crystal structures of low-melting ionic transition-metal complexes with N-alkylimidazole ligands
• Authors of publication: Vander Hoogerstraete, Tom; Brooks, Neil R.; Norberg, Bernadette; Wouters, Johan; Van Hecke, Kristof; Van Meervelt, Luc; Binnemans, Koen
• Journal of publication: CrystEngComm
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 15
• Pages of publication: 4902
• a: 8.2018 ± 0.0002 Å
• b: 20.3183 ± 0.0005 Å
• c: 26.938 ± 0.0008 Å
• α: 90°
• β: 92.341 ± 0.003°
• γ: 90°
• Cell volume: 4485.4 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0593
• Residual factor for significantly intense reflections: 0.0466
• Weighted residual factors for significantly intense reflections: 0.1187
• Weighted residual factors for all reflections included in the refinement: 0.1225
• Goodness-of-fit parameter for all reflections included in the refinement: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No