Information card for entry 7208688

Structure parameters

• Common name: (Ni(Ni(4,4'dtbpy)(H2O))8(W(CN)8)6)*17H2O
• Chemical name: {Ni[Ni(4,4'dtbpy)(H2O)]8[W(CN)8]6}*17H2O
• Formula: C208 H232 N64 Ni9 O23 W6
• Calculated formula: C208 H232 N64 Ni9 O23 W6
• Title of publication: Geometrical isomerism in pentadecanuclear high-spin Ni9W6 clusters with symmetrical bidentate ligands detected
• Authors of publication: Nowicka, Beata; Stadnicka, Katarzyna; Nitek, Wojciech; Rams, Michał; Sieklucka, Barbara
• Journal of publication: CrystEngComm
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 20
• Pages of publication: 6559
• a: 20.2904 ± 0.0002 Å
• b: 20.3359 ± 0.0002 Å
• c: 21.3903 ± 0.0003 Å
• α: 105.6°
• β: 111.614 ± 0.001°
• γ: 98.081 ± 0.001°
• Cell volume: 7615.02 ± 0.17 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1047
• Residual factor for significantly intense reflections: 0.054
• Weighted residual factors for significantly intense reflections: 0.123
• Weighted residual factors for all reflections included in the refinement: 0.1534
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No