Information card for entry 7208989

Structure parameters

• Formula: C56 H46 N8 Ni O22.5 Ta
• Calculated formula: C56 H37 N8 Ni O22.511 Ta
• Title of publication: A series of compounds containing various (oxalato)tantalate(v) complex anions ‒ synthesis, properties and the mixed-metal oxide formation via thermal decomposition
• Authors of publication: Androš, Lidija; Matković-Čalogović, Dubravka; Planinić, Pavica
• Journal of publication: CrystEngComm
• Year of publication: 2013
• Journal volume: 15
• Journal issue: 3
• Pages of publication: 533
• a: 12.0511 ± 0.0004 Å
• b: 14.9625 ± 0.0005 Å
• c: 16.2348 ± 0.0005 Å
• α: 76.487 ± 0.003°
• β: 86.836 ± 0.003°
• γ: 72.44 ± 0.003°
• Cell volume: 2713.33 ± 0.16 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0752
• Residual factor for significantly intense reflections: 0.0586
• Weighted residual factors for significantly intense reflections: 0.1315
• Weighted residual factors for all reflections included in the refinement: 0.1356
• Goodness-of-fit parameter for all reflections included in the refinement: 1.143
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No