Information card for entry 7209061

Structure parameters

• Formula: C50 H55 B N10 Ni2 O47 W12
• Calculated formula: C50 H40 B N10 Ni2 O47 W12
• Title of publication: The syntheses, structures and characterizations of a series of frameworks constructed from polyoxometalates, metals and organic units
• Authors of publication: Wang, Yan; Wang, La-Mei; Li, Zhi-Fang; Hu, Yang-Yang; Li, Guang-Hua; Xiao, Li-Na; Wang, Tie-gang; Zheng, Da-Fang; Cui, Xiao-Bing; Xu, Ji-Qing
• Journal of publication: CrystEngComm
• Year of publication: 2013
• Journal volume: 15
• Journal issue: 2
• Pages of publication: 285
• a: 13.292 ± 0.003 Å
• b: 15.146 ± 0.003 Å
• c: 19.946 ± 0.004 Å
• α: 90°
• β: 102.23 ± 0.03°
• γ: 90°
• Cell volume: 3924.4 ± 1.5 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0993
• Residual factor for significantly intense reflections: 0.0646
• Weighted residual factors for significantly intense reflections: 0.127
• Weighted residual factors for all reflections included in the refinement: 0.1468
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No