Information card for entry 7210305

Structure parameters

• Formula: C10 H104 As4 N2 Na10 O199 Tb6 W44
• Calculated formula: C10 H18 As4 N2 Na10 O199 Tb6 W44
• Title of publication: Assembly of chainlike polyoxometalate-based lanthanide complexes in one-pot reaction system
• Authors of publication: Feng, Xiao-Jia; Han, Hua-Yan; Wang, Yong-Hui; Li, Lu-Lu; Li, Yang-Guang; Wang, En-Bo
• Journal of publication: CrystEngComm
• Year of publication: 2013
• Journal volume: 15
• Journal issue: 36
• Pages of publication: 7267
• a: 13.085 ± 0.003 Å
• b: 19.689 ± 0.004 Å
• c: 22.821 ± 0.005 Å
• α: 104.33 ± 0.03°
• β: 95.37 ± 0.03°
• γ: 104.76 ± 0.03°
• Cell volume: 5431 ± 2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1438
• Residual factor for significantly intense reflections: 0.0865
• Weighted residual factors for significantly intense reflections: 0.1569
• Weighted residual factors for all reflections included in the refinement: 0.1729
• Goodness-of-fit parameter for all reflections included in the refinement: 1.045
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No