Information card for entry 7210587

Structure parameters

• Formula: C14 H72 Cu3 Ge N12 O51.5 Tb W11
• Calculated formula: C14 H51 Cu3 Ge N12 O51.5 Tb W11
• Title of publication: Organic‒inorganic hybrids based on monovacant Keggin-type polyoxotungstates and 3d‒4f heterometals
• Authors of publication: Zhao, Hai-Yan; Zhao, Jun-Wei; Yang, Bai-Feng; He, Huan; Yang, Guo-Yu
• Journal of publication: CrystEngComm
• Year of publication: 2013
• Journal volume: 15
• Journal issue: 40
• Pages of publication: 8186
• a: 46.988 ± 0.003 Å
• b: 12.2367 ± 0.0003 Å
• c: 23.1895 ± 0.0006 Å
• α: 90°
• β: 104.813 ± 0.004°
• γ: 90°
• Cell volume: 12890.3 ± 1 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0986
• Residual factor for significantly intense reflections: 0.0717
• Weighted residual factors for significantly intense reflections: 0.1811
• Weighted residual factors for all reflections included in the refinement: 0.2014
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No