Information card for entry 7210795

Structure parameters

• Formula: C24 H24 N3 Ni O8
• Calculated formula: C21.809 H22.427 N3 Ni O8
• Title of publication: Host‒guest chemistry of NiII coordination compounds with PDC and (py)2CO: reversible crystal-to-amorphous transformations induced by solvent exchange
• Authors of publication: Calderón-Casado, Ainhoa; Barandika, Gotzone; Bazán, Begoña; Urtiaga, Miren-Karmele; Arriortua, María-Isabel
• Journal of publication: CrystEngComm
• Year of publication: 2013
• Journal volume: 15
• Journal issue: 25
• Pages of publication: 5134
• a: 8.447 ± 0.004 Å
• b: 11.013 ± 0.006 Å
• c: 14.285 ± 0.006 Å
• α: 107.72 ± 0.03°
• β: 100.94 ± 0.02°
• γ: 97.82 ± 0.03°
• Cell volume: 1215.9 ± 1.1 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Method of determination: powder diffraction
• Diffraction radiation wavelength: 1.54051 Å
• Diffraction radiation type: X-ray
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No