Crystallography Open Database

Information card for entry 7211229

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Coordinates	7211229.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H14 Cl2 N4 Pb
Calculated formula	C14 H14 Cl2 N4 Pb
Title of publication	Solid state structural transformation of 1D to intermediate 2D and then to 3D porous coordination polymer by anion replacement; new precursors for preparation of PbCl2, Pb3O2Cl2 and PbO nanoparticles
Authors of publication	Hashemi, Lida; Morsali, Ali
Journal of publication	CrystEngComm
Year of publication	2013
Journal volume	15
Journal issue	44
Pages of publication	8894
a	12.805 ± 0.001 Å
b	4.0989 ± 0.0003 Å
c	16.246 ± 0.001 Å
α	90°
β	96.729 ± 0.001°
γ	90°
Cell volume	846.82 ± 0.1 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	5
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/c 1
Hall space group symbol	-P 2yc
Residual factor for all reflections	0.0157
Residual factor for significantly intense reflections	0.0155
Weighted residual factors for significantly intense reflections	0.0388
Weighted residual factors for all reflections included in the refinement	0.0389
Goodness-of-fit parameter for all reflections included in the refinement	1.06
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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