Information card for entry 7212221

Structure parameters

• Formula: C27 H24 N6 O19 Pb4
• Calculated formula: C27 H12 N6 O19 Pb4
• Title of publication: 4-Carboxylphthalhydrazidate-bridged layered Pb(ii) coordination polymers
• Authors of publication: Jin, Juan; Jia, Ming-Jun; Peng, Yu; Hou, Qin; Yu, Jie-Hui; Xu, Ji-Qing
• Journal of publication: CrystEngComm
• Year of publication: 2010
• Journal volume: 12
• Journal issue: 6
• Pages of publication: 1850
• a: 10.594 ± 0.002 Å
• b: 10.716 ± 0.002 Å
• c: 14.99 ± 0.003 Å
• α: 85.91 ± 0.03°
• β: 80.52 ± 0.03°
• γ: 89.68 ± 0.03°
• Cell volume: 1674.2 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0457
• Residual factor for significantly intense reflections: 0.0384
• Weighted residual factors for significantly intense reflections: 0.106
• Weighted residual factors for all reflections included in the refinement: 0.1105
• Goodness-of-fit parameter for all reflections included in the refinement: 1.113
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No