Information card for entry 7212776

Structure parameters

• Formula: H150 K12 O239 P6 Rb6 V8 W39
• Calculated formula: K11.982 O203 P6 Rb6 V8 W39
• Title of publication: Mixed-valent vanadium substituted polyoxometalates: the wheel shaped [Rb3⊂{VVVIV3O7(H2O)6}2{H6P6W39O147(H2O)3}]15−
• Authors of publication: Assran, Awatef S.; Izarova, Natalya V.; Kortz, Ulrich
• Journal of publication: CrystEngComm
• Year of publication: 2010
• Journal volume: 12
• Journal issue: 10
• Pages of publication: 2684
• a: 22.9885 ± 0.0013 Å
• b: 22.9885 ± 0.0013 Å
• c: 21.3679 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 9779.4 ± 1 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 190
• Hermann-Mauguin space group symbol: P -6 2 c
• Hall space group symbol: P -6c -2c
• Residual factor for all reflections: 0.0574
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.105
• Weighted residual factors for all reflections included in the refinement: 0.1128
• Goodness-of-fit parameter for all reflections included in the refinement: 1.104
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No