Information card for entry 7212840

Structure parameters

• Formula: C36 H37 Cl2 N13 O9 Pb
• Calculated formula: C36 H37 Cl2 N13 O9 Pb
• Title of publication: Lead(ii) complexes of bis- and tris-bidentate compartmental ligands based on pyridyl-pyrazole and pyridyl-triazole fragments: coordination networks and a discrete dimeric box
• Authors of publication: Najar, Adel M.; Tidmarsh, Ian S.; Ward, Michael D.
• Journal of publication: CrystEngComm
• Year of publication: 2010
• Journal volume: 12
• Journal issue: 11
• Pages of publication: 3642
• a: 17.4206 ± 0.0004 Å
• b: 22.1469 ± 0.0005 Å
• c: 24.5102 ± 0.0007 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 9456.3 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for all reflections: 0.0936
• Residual factor for significantly intense reflections: 0.0623
• Weighted residual factors for significantly intense reflections: 0.1709
• Weighted residual factors for all reflections included in the refinement: 0.1832
• Goodness-of-fit parameter for all reflections included in the refinement: 1.123
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No