Information card for entry 7212842

Structure parameters

• Formula: C49 H47 Cl4 N17 O22 Pb2
• Calculated formula: C49 H47 Cl4 N17 O22 Pb2
• Title of publication: Lead(ii) complexes of bis- and tris-bidentate compartmental ligands based on pyridyl-pyrazole and pyridyl-triazole fragments: coordination networks and a discrete dimeric box
• Authors of publication: Najar, Adel M.; Tidmarsh, Ian S.; Ward, Michael D.
• Journal of publication: CrystEngComm
• Year of publication: 2010
• Journal volume: 12
• Journal issue: 11
• Pages of publication: 3642
• a: 11.6268 ± 0.0006 Å
• b: 12.1895 ± 0.0006 Å
• c: 13.5805 ± 0.0007 Å
• α: 102.909 ± 0.003°
• β: 102.681 ± 0.003°
• γ: 102.962 ± 0.002°
• Cell volume: 1753.04 ± 0.16 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0946
• Residual factor for significantly intense reflections: 0.0584
• Weighted residual factors for significantly intense reflections: 0.1423
• Weighted residual factors for all reflections included in the refinement: 0.161
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No