Structural and conformational studies of alcohol, diol and methyl ether derivatives of dibenzo-14-crown-4. Implications for ligand and tecton design
Authors of publication
Olsher, Uriel; Shoham, Gil; Dalley, N. Kent; Weining, Jiang; Luboch, Elzbieta; Yu, Zong-Yuan; Knobeloch, John M.; Lee, Jong Chan; Talanov, Vladimir S.; Bartsch, Richard A.
Journal of publication
Journal of the Chemical Society, Perkin Transactions 2
Year of publication
1999
Journal issue
11
Pages of publication
2557
a
33.139 ± 0.008 Å
b
5.064 ± 0.001 Å
c
20.155 ± 0.003 Å
α
90°
β
108.3 ± 0.02°
γ
90°
Cell volume
3211.3 ± 1.2 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
3
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.0986
Residual factor for significantly intense reflections
0.0492
Weighted residual factors for all reflections
0.1168
Weighted residual factors for significantly intense reflections
0.1021
Goodness-of-fit parameter for all reflections
0.981
Goodness-of-fit parameter for significantly intense reflections
