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Information card for entry 7213254
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Jmol._Canvas2D (Jmol) "jmolApplet0"[x]
Coordinates | 7213254.cif |
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Original paper (by DOI) | HTML |
Common name | Bridged (beta-alkoxyalkyl)Co(III)salen |
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Formula | C23 H27 Cl2 Co N2 O4 |
Calculated formula | C23 H27 Cl2 Co N2 O4 |
Title of publication | Bridged (β-alkoxyalkyl)CoIII(salen) complexes by intramolecular alkoxycobaltation of unactivated alkenes: new models for coenzyme B12 |
Authors of publication | Blaauw, Rolf; Kingma, Irene E.; Laan, Jan H.; van der Baan, Juul L.; Balt, Sijbe; de Bolster, Martinus W. G.; Klumpp, Gerhard W.; Smeets, Wilberth J. J.; Spek, Anthony L. |
Journal of publication | Journal of the Chemical Society, Perkin Transactions 1 |
Year of publication | 2000 |
Journal issue | 8 |
Pages of publication | 1199 |
a | 12.4467 ± 0.0014 Å |
b | 11.4978 ± 0.0007 Å |
c | 19.0943 ± 0.0018 Å |
α | 90° |
β | 125.34 ± 0.007° |
γ | 90° |
Cell volume | 2229.1 ± 0.4 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 6 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.1424 |
Residual factor for significantly intense reflections | 0.0655 |
Weighted residual factors for significantly intense reflections | 0.1062 |
Weighted residual factors for all reflections included in the refinement | 0.1327 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.017 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/7213254.html
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