Information card for entry 7213449

Structure parameters

• Formula: C36 H48 N2 Si
• Calculated formula: C36 H48 N2 Si
• SMILES: [Si]1(N2C=CC=CC2=C2N1[C@H]1[C@@H](C2)CCC1)(c1c(cc(cc1C)C)C)c1c(cc(cc1C(C)C)C(C)C)C(C)C
• Title of publication: Utilization of industrial waste materials. Part 20. Stereoselective cycloaddition of silylenes and a disilene to an enantiomerically pure cyclic ketimine derived from an industrial waste material
• Authors of publication: von Keyserlingk, Nikolai Graf; Martens, Jürgen; Ostendorf, Detlev; Saak, Wolfgang; Weidenbruch, Manfred
• Journal of publication: Journal of the Chemical Society, Perkin Transactions 1
• Year of publication: 2001
• Journal issue: 7
• Pages of publication: 706
• a: 9.7011 ± 0.0005 Å
• b: 11.704 ± 0.0008 Å
• c: 14.5936 ± 0.001 Å
• α: 96.862 ± 0.008°
• β: 100.249 ± 0.007°
• γ: 100.163 ± 0.007°
• Cell volume: 1585.37 ± 0.19 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 4
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.1156
• Residual factor for significantly intense reflections: 0.0486
• Weighted residual factors for significantly intense reflections: 0.0874
• Weighted residual factors for all reflections included in the refinement: 0.1025
• Goodness-of-fit parameter for all reflections included in the refinement: 0.792
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No