Information card for entry 7213775

Structure parameters

• Formula: C68 H48 Cu4 Mo12 N12 O42 Si V2
• Calculated formula: C68 H48 Cu4 Mo12 N12 O42 Si V2
• Title of publication: The design, syntheses and characterization of a series of hybrids based on polyoxometalates and metal complexes
• Authors of publication: Wang, La-Mei; Wang, Yan; Fan, Yong; Xiao, Li-Na; Hu, Yang-Yang; Gao, Zhong-Min; Zheng, Da-Fang; Cui, Xiao-Bing; Xu, Ji-Qing
• Journal of publication: CrystEngComm
• Year of publication: 2014
• Journal volume: 16
• Journal issue: 3
• Pages of publication: 430
• a: 13.2145 ± 0.0011 Å
• b: 24.934 ± 0.002 Å
• c: 27.184 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8956.9 ± 1.2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 8
• Space group number: 72
• Hermann-Mauguin space group symbol: I b a m
• Hall space group symbol: -I 2 2c
• Residual factor for all reflections: 0.0716
• Residual factor for significantly intense reflections: 0.0518
• Weighted residual factors for significantly intense reflections: 0.1347
• Weighted residual factors for all reflections included in the refinement: 0.1477
• Goodness-of-fit parameter for all reflections included in the refinement: 1.046
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No