Anhydrates and/or hydrates in nitrate, sulphate and phosphate salts of 4-aminopyridine, (4-AP) and 3,4-diaminopyridine (3,4-DAP): the role of the water molecules in the hydrates
Authors of publication
Hursthouse, Michael B.; Montis, Riccardo; Niitsoo, Liisa; Sarson, Jonathan; Threlfall, Terence L.; Asiri, Abdullah Mohamed; Khan, Salman Ahmad; Obaid, Abdullah Yousef; Al-Harbi, Laila Mohammad
Journal of publication
CrystEngComm
Year of publication
2014
Journal volume
16
Journal issue
11
Pages of publication
2205
a
6.4515 ± 0.0002 Å
b
8.4229 ± 0.0002 Å
c
12.4728 ± 0.0008 Å
α
96.429 ± 0.007°
β
97.523 ± 0.007°
γ
95.349 ± 0.007°
Cell volume
663.7 ± 0.05 Å3
Cell temperature
120 ± 2 K
Ambient diffraction temperature
120 ± 2 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0375
Residual factor for significantly intense reflections
0.0326
Weighted residual factors for significantly intense reflections
0.1001
Weighted residual factors for all reflections included in the refinement
0.1134
Goodness-of-fit parameter for all reflections included in the refinement
