Information card for entry 7214644

Structure parameters

• Formula: C38.32 H43.32 B4 Cu4 F16 N13 O0.33
• Calculated formula: C38.32 H43.32 B4 Cu4 F16 N13 O0.33
• Title of publication: Structural controls of 2D sheet copper(i) ethylene and carbonyl coordination polymers directed by anions and solvents
• Authors of publication: Maekawa, Masahiko; Tominaga, Toshi; Sugimoto, Kunihisa; Okubo, Takashi; Kuroda‒Sowa, Takayoshi; Munakata, Megumu; Kitagawa, Susumu
• Journal of publication: CrystEngComm
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 18
• Pages of publication: 5955
• a: 14.0511 ± 0.0008 Å
• b: 14.0511 ± 0.0008 Å
• c: 22.6054 ± 0.0016 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 3865.1 ± 0.4 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 7
• Space group number: 146
• Hermann-Mauguin space group symbol: R 3 :H
• Hall space group symbol: R 3
• Residual factor for all reflections: 0.0273
• Residual factor for significantly intense reflections: 0.0272
• Weighted residual factors for significantly intense reflections: 0.0722
• Weighted residual factors for all reflections included in the refinement: 0.0723
• Goodness-of-fit parameter for all reflections included in the refinement: 1.106
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No