Information card for entry 7214646

Structure parameters

• Formula: C37 H30 Cu4 F24 N14 O3 P4
• Calculated formula: C37 H35.94 Cu4 F24 N14 O3 P4
• Title of publication: Structural controls of 2D sheet copper(i) ethylene and carbonyl coordination polymers directed by anions and solvents
• Authors of publication: Maekawa, Masahiko; Tominaga, Toshi; Sugimoto, Kunihisa; Okubo, Takashi; Kuroda‒Sowa, Takayoshi; Munakata, Megumu; Kitagawa, Susumu
• Journal of publication: CrystEngComm
• Year of publication: 2012
• Journal volume: 14
• Journal issue: 18
• Pages of publication: 5955
• a: 14.3797 ± 0.0015 Å
• b: 14.3797 ± 0.0015 Å
• c: 23.083 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 4133.5 ± 0.8 ų
• Cell temperature: 120 ± 2 K
• Ambient diffraction temperature: 120 ± 2 K
• Number of distinct elements: 7
• Space group number: 146
• Hermann-Mauguin space group symbol: R 3 :H
• Hall space group symbol: R 3
• Residual factor for all reflections: 0.0639
• Residual factor for significantly intense reflections: 0.0567
• Weighted residual factors for significantly intense reflections: 0.1198
• Weighted residual factors for all reflections included in the refinement: 0.1231
• Goodness-of-fit parameter for all reflections included in the refinement: 1.076
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No