Information card for entry 7216551

Structure parameters

• Formula: Cu8 H152 Mo30 N20 O169 V10
• Calculated formula: Cu8 Mo30 N18 O160 V10
• Title of publication: Multidimensional all-inorganic frameworks based on new molybdovanadate cluster of [VMo7O28]9−with Cu(ii) linker showing semiconducting behavior
• Authors of publication: Gao, Qiao; Li, Fengyan; Sun, Minghui; Xu, Lin; Wang, Yuchao; Bai, Jie
• Journal of publication: CrystEngComm
• Year of publication: 2014
• Journal volume: 16
• Journal issue: 33
• Pages of publication: 7681
• a: 14.7333 ± 0.0003 Å
• b: 17.2359 ± 0.0006 Å
• c: 18.2871 ± 0.0004 Å
• α: 96.789 ± 0.002°
• β: 98.188 ± 0.002°
• γ: 93.537 ± 0.002°
• Cell volume: 4549.7 ± 0.2 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0636
• Residual factor for significantly intense reflections: 0.0453
• Weighted residual factors for significantly intense reflections: 0.1245
• Weighted residual factors for all reflections included in the refinement: 0.135
• Goodness-of-fit parameter for all reflections included in the refinement: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No