Information card for entry 7216575

Structure parameters

• Formula: C64 H88 As2 N4 O36 V10
• Calculated formula: C64 H88 As2 N4 O36 V10
• Title of publication: The first example of a novel one-dimensional cyclic tetrameric metavanadate: [PPh4]2V4O11
• Authors of publication: Sharma, Sanjeev; Ramanan, Arunachalam; Zavalij, Peter Y.; Whittingham, M. Stanley
• Journal of publication: CrystEngComm
• Year of publication: 2002
• Journal volume: 4
• Journal issue: 100
• Pages of publication: 601
• a: 10.4005 ± 0.0004 Å
• b: 11.8621 ± 0.0005 Å
• c: 17.3981 ± 0.0007 Å
• α: 97.621 ± 0.001°
• β: 90.256 ± 0.001°
• γ: 111.417 ± 0.001°
• Cell volume: 1977.31 ± 0.14 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0412
• Residual factor for significantly intense reflections: 0.0338
• Weighted residual factors for significantly intense reflections: 0.0862
• Weighted residual factors for all reflections included in the refinement: 0.0901
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No