Information card for entry 7216753

Structure parameters

• Formula: C24 H31 Cl4 N2 Pd Sb
• Calculated formula: C24 H31 Cl4 N2 Pd Sb
• SMILES: c12c(cccc1)C[N](C)(C)[Sb]2(c1ccccc1)(Cl)[Pd](Cl)(Cl)Cl.c1(ccccc1)C[NH+](C)C
• Title of publication: Palladium(ii) complexes with chiral organoantimony(iii) ligands. Solution behaviour and solid state structures
• Authors of publication: Copolovici, Dana; Isaia, Francesco; Breunig, Hans J.; Raţ, Ciprian I.; Silvestru, Cristian
• Journal of publication: RSC Advances
• Year of publication: 2014
• Journal volume: 4
• Journal issue: 51
• Pages of publication: 26569
• a: 8.7797 ± 0.0009 Å
• b: 10.3772 ± 0.0011 Å
• c: 15.8911 ± 0.0017 Å
• α: 98.954 ± 0.002°
• β: 102.05 ± 0.002°
• γ: 96.987 ± 0.002°
• Cell volume: 1380.7 ± 0.3 ų
• Cell temperature: 297 ± 2 K
• Ambient diffraction temperature: 297 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0797
• Residual factor for significantly intense reflections: 0.0648
• Weighted residual factors for significantly intense reflections: 0.1129
• Weighted residual factors for all reflections included in the refinement: 0.1175
• Goodness-of-fit parameter for all reflections included in the refinement: 1.249
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No