Information card for entry 7217124

Structure parameters

• Formula: C28 H44 Ag4 N24 Na O41 P W12
• Calculated formula: C28 H44 Ag4 N24 Na O41 P W12
• Title of publication: Two unusual organic‒inorganic hybrid 3-D frameworks based on Keggin-type heteropoly blue anion-chains, 40-membered macrocycles, and sodium linker units
• Authors of publication: Zhang, He; Yu, Kai; Gao, Song; Wang, Chun-Mei; Wang, Chun-Xiao; Wang, Hai-Yan; Zhou, Bai-Bin
• Journal of publication: CrystEngComm
• Year of publication: 2014
• Journal volume: 16
• Journal issue: 36
• Pages of publication: 8449
• a: 10.9694 ± 0.0011 Å
• b: 13.6637 ± 0.0014 Å
• c: 13.9341 ± 0.0014 Å
• α: 64.8306 ± 0.0013°
• β: 73.1694 ± 0.0015°
• γ: 69.7887 ± 0.0015°
• Cell volume: 1748.6 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0513
• Residual factor for significantly intense reflections: 0.0659
• Weighted residual factors for significantly intense reflections: 0.0942
• Weighted residual factors for all reflections included in the refinement: 0.1076
• Goodness-of-fit parameter for all reflections included in the refinement: 1.167
• Diffraction radiation wavelength: 0.71 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No