Information card for entry 7217519

Structure parameters

• Formula: Cu11 H144 Mo30 N10 Na O181 V9
• Calculated formula: Cu11 Mo30 N7 Na O177 V9
• Title of publication: Multidimensional all-inorganic frameworks based on new molybdovanadate cluster of [VMo7O28]9−with Cu(ii) linker showing semiconducting behavior
• Authors of publication: Gao, Qiao; Li, Fengyan; Sun, Minghui; Xu, Lin; Wang, Yuchao; Bai, Jie
• Journal of publication: CrystEngComm
• Year of publication: 2014
• Journal volume: 16
• Journal issue: 33
• Pages of publication: 7681
• a: 53.884 ± 0.005 Å
• b: 13.9563 ± 0.0011 Å
• c: 26.848 ± 0.002 Å
• α: 90°
• β: 104.181 ± 0.002°
• γ: 90°
• Cell volume: 19575 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1068
• Residual factor for significantly intense reflections: 0.0663
• Weighted residual factors for significantly intense reflections: 0.1907
• Weighted residual factors for all reflections included in the refinement: 0.215
• Goodness-of-fit parameter for all reflections included in the refinement: 1.004
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Duplicate of: 7216552
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No