Information card for entry 7218512

Structure parameters

• Formula: C14 H126 As6 Ce4 K14 Li4 N2 O264 W58
• Calculated formula: C14 H6 As6 Ce4 K14 N2 O246 W58
• Title of publication: From a versatile arsenotungstate precursor to a large lanthanide-containing polyoxometalate‒carboxylate hybrid
• Authors of publication: Li, Suzhi; Wang, Yuan; Ma, Pengtao; Wang, Jingping; Niu, Jingyang
• Journal of publication: CrystEngComm
• Year of publication: 2014
• Journal volume: 16
• Journal issue: 47
• Pages of publication: 10746
• a: 19.568 ± 0.002 Å
• b: 20.952 ± 0.002 Å
• c: 23.623 ± 0.003 Å
• α: 74.831 ± 0.002°
• β: 86.481 ± 0.002°
• γ: 64.269 ± 0.002°
• Cell volume: 8405.6 ± 1.6 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.135
• Residual factor for significantly intense reflections: 0.0796
• Weighted residual factors for significantly intense reflections: 0.1833
• Weighted residual factors for all reflections included in the refinement: 0.2001
• Goodness-of-fit parameter for all reflections included in the refinement: 1.078
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No