Information card for entry 7218719

Structure parameters

• Formula: C32 H26 Cl N3 O5
• Calculated formula: C32 H26 Cl N3 O5
• Title of publication: One-pot synthesis of 6,11-dihydro-5H-indolizino[8,7-b]indoles via sequential formation of β-enamino ester, Michael addition and Pictet-Spengler reactions
• Authors of publication: Yan, Chao Guo; Zhu, Dan; Sun, Jing
• Journal of publication: RSC Adv.
• Year of publication: 2014
• a: 9.634 ± 0.002 Å
• b: 19.608 ± 0.005 Å
• c: 15.793 ± 0.004 Å
• α: 90°
• β: 105.544 ± 0.007°
• γ: 90°
• Cell volume: 2874.2 ± 1.2 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1896
• Residual factor for significantly intense reflections: 0.0641
• Weighted residual factors for significantly intense reflections: 0.135
• Weighted residual factors for all reflections included in the refinement: 0.1756
• Goodness-of-fit parameter for all reflections included in the refinement: 0.995
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No