Information card for entry 7219348

Structure parameters

• Formula: C148 H142 Cl Ir4 N20 O37 Pb2
• Calculated formula: C148 H142 Cl Ir4 N20 O37 Pb2
• Title of publication: Four new lead(ii)‒iridium(iii) heterobimetallic coordination frameworks: synthesis, structures, luminescence and oxygen-sensing properties
• Authors of publication: Chen, Yi-Ting; Lin, Chun-Yen; Lee, Gene-Hsiang; Ho, Mei-Lin
• Journal of publication: CrystEngComm
• Year of publication: 2015
• Journal volume: 17
• Journal issue: 10
• Pages of publication: 2129
• a: 29.4296 ± 0.0007 Å
• b: 8.7352 ± 0.0002 Å
• c: 30.6568 ± 0.0007 Å
• α: 90°
• β: 99.2586 ± 0.0007°
• γ: 90°
• Cell volume: 7778.4 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.0539
• Residual factor for significantly intense reflections: 0.0429
• Weighted residual factors for significantly intense reflections: 0.1263
• Weighted residual factors for all reflections included in the refinement: 0.1368
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No