Crystallography Open Database

Information card for entry 7221646

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Coordinates	7221646.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C56 H24 F24 N4 O16 Rh4
Calculated formula	C56 F24 N4 O16 Rh4
Title of publication	Crystal-to-crystal transformation of fishnet-like layered compounds: a self-locking structure with position-variable intercalated molecules
Authors of publication	Nishio, Masaki; Motokawa, Natsuko; Miyasaka, Hitoshi
Journal of publication	CrystEngComm
Year of publication	2015
Journal volume	17
Journal issue	40
Pages of publication	7618
a	10.214 ± 0.003 Å
b	14.064 ± 0.003 Å
c	14.282 ± 0.004 Å
α	75.127 ± 0.011°
β	87.917 ± 0.012°
γ	79.52 ± 0.013°
Cell volume	1949.7 ± 0.9 Å³
Cell temperature	97 K
Ambient diffraction temperature	97 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1847
Residual factor for significantly intense reflections	0.1064
Weighted residual factors for significantly intense reflections	0.2782
Weighted residual factors for all reflections included in the refinement	0.3529
Goodness-of-fit parameter for all reflections included in the refinement	1.035
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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