Information card for entry 7221777

Structure parameters

• Formula: C116 H130 Cl1.5 Dy2 F24 N9.5 O18
• Calculated formula: C116 H130 Cl1.5 Dy2 F24 N9.5 O18
• Title of publication: Crystallization of triple- and quadruple-stranded dinuclear bis-β-diketonate-Dy(iii) helicates: single molecule magnetic behavior
• Authors of publication: Chen, Peng; Li, Hongfeng; Sun, Wenbin; Tang, Jinkui; Zhang, Lei; Yan, Pengfei
• Journal of publication: CrystEngComm
• Year of publication: 2015
• Journal volume: 17
• Journal issue: 37
• Pages of publication: 7227
• a: 45.2139 ± 0.0005 Å
• b: 20.4624 ± 0.0002 Å
• c: 28.0974 ± 0.0003 Å
• α: 90°
• β: 100.59 ± 0.0012°
• γ: 90°
• Cell volume: 25552.5 ± 0.5 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0742
• Residual factor for significantly intense reflections: 0.0593
• Weighted residual factors for significantly intense reflections: 0.1665
• Weighted residual factors for all reflections included in the refinement: 0.1802
• Goodness-of-fit parameter for all reflections included in the refinement: 1.028
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No