Information card for entry 7223090

Structure parameters

• Formula: C56 H86 Br2 Li2 N3 O4 Si2 Sm
• Calculated formula: C56 H86 Br2 Li2 N3 O4 Si2 Sm
• Title of publication: Anionic phenoxy-amido rare-earth complexes as efficient catalysts for amidation of aldehydes with amines
• Authors of publication: Wang, Chao; Huang, Ling ling; Lu, Min; Zhao, Bei; Wang, Yaorong; Zhang, Yong; Shen, Qi; Yao, Yingming
• Journal of publication: RSC Adv.
• Year of publication: 2015
• a: 21.6583 ± 0.0016 Å
• b: 21.6583 ± 0.0016 Å
• c: 26.562 ± 0.003 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 12459.8 ± 1.9 ų
• Cell temperature: 223 ± 2 K
• Ambient diffraction temperature: 223 ± 2 K
• Number of distinct elements: 8
• Space group number: 110
• Hermann-Mauguin space group symbol: I 41 c d
• Hall space group symbol: I 4bw -2c
• Residual factor for all reflections: 0.0873
• Residual factor for significantly intense reflections: 0.068
• Weighted residual factors for significantly intense reflections: 0.0986
• Weighted residual factors for all reflections included in the refinement: 0.1041
• Goodness-of-fit parameter for all reflections included in the refinement: 1.24
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No