Information card for entry 7224056

Structure parameters

• Formula: C24 H66 K4 Nb6 O33 Rh2
• Calculated formula: C24 H36 K4 Nb6 O33 Rh2
• Title of publication: Unique solubility of polyoxoniobate salts in methanol: coordination to cations and POM methylation
• Authors of publication: Abramov, Pavel A.; Vicent, Cristian; Kompankov, Nikolay B.; Laricheva, Yuliya A.; Sokolov, Maksim Nailyevich
• Journal of publication: RSC Adv.
• Year of publication: 2016
• a: 14.6139 ± 0.0005 Å
• b: 9.3769 ± 0.0003 Å
• c: 19.9504 ± 0.0005 Å
• α: 90°
• β: 95.964 ± 0.001°
• γ: 90°
• Cell volume: 2719.07 ± 0.14 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0617
• Residual factor for significantly intense reflections: 0.0398
• Weighted residual factors for significantly intense reflections: 0.1143
• Weighted residual factors for all reflections included in the refinement: 0.157
• Goodness-of-fit parameter for all reflections included in the refinement: 1.143
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No