Information card for entry 7224229

Structure parameters

• Chemical name: 6
• Formula: C30 H50 N6 Ni O19 Zn
• Calculated formula: C30 H34 N6 Ni O19 Zn
• Title of publication: Two-step synthesis of heterometallic coordination polymers using a polyazamacrocyclic linker
• Authors of publication: Aríñez-Soriano, J.; Albalad, J.; Pérez-Carvajal, J.; Imaz, I.; Busqué, F.; Juanhuix, J.; Maspoch, D.
• Journal of publication: CrystEngComm
• Year of publication: 2016
• Journal volume: 18
• Journal issue: 22
• Pages of publication: 4196
• a: 11.36 ± 0.003 Å
• b: 22.08 ± 0.003 Å
• c: 15.56 ± 0.003 Å
• α: 90°
• β: 90.2 ± 0.03°
• γ: 90°
• Cell volume: 3902.9 ± 1.4 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1127
• Residual factor for significantly intense reflections: 0.1057
• Weighted residual factors for significantly intense reflections: 0.3426
• Weighted residual factors for all reflections included in the refinement: 0.3522
• Goodness-of-fit parameter for all reflections included in the refinement: 1.669
• Diffraction radiation wavelength: 0.70109 Å
• Diffraction radiation type: synchrotronradiation
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No