Information card for entry 7224252

Structure parameters

• Formula: C47 H67 Gd N2 O6
• Calculated formula: C47 H67 Gd N2 O6
• Title of publication: Heteroleptic lanthanide amides complexes bearing carbon-bridged bis(phenolate) ligands: synthesis, structure and their application in the polymerization of ε-caprolactone
• Authors of publication: Zhou, Yanxu; Shen, Yingzhong; Zhao, Jing; Wang, Yulong; Peng, Ling; Tao, Xian
• Journal of publication: RSC Adv.
• Year of publication: 2016
• a: 13.348 ± 0.002 Å
• b: 14.064 ± 0.003 Å
• c: 16.293 ± 0.003 Å
• α: 75.129 ± 0.002°
• β: 69.752 ± 0.002°
• γ: 62.759 ± 0.002°
• Cell volume: 2533.6 ± 0.8 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0735
• Residual factor for significantly intense reflections: 0.0594
• Weighted residual factors for significantly intense reflections: 0.1948
• Weighted residual factors for all reflections included in the refinement: 0.2048
• Goodness-of-fit parameter for all reflections included in the refinement: 1.051
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No