Information card for entry 7224254

Structure parameters

• Formula: C53 H79 Gd N2 O6
• Calculated formula: C53 H79 Gd N2 O6
• Title of publication: Heteroleptic lanthanide amides complexes bearing carbon-bridged bis(phenolate) ligands: synthesis, structure and their application in the polymerization of ε-caprolactone
• Authors of publication: Zhou, Yanxu; Shen, Yingzhong; Zhao, Jing; Wang, Yulong; Peng, Ling; Tao, Xian
• Journal of publication: RSC Adv.
• Year of publication: 2016
• a: 13.74 ± 0.002 Å
• b: 20.389 ± 0.004 Å
• c: 18.914 ± 0.003 Å
• α: 90°
• β: 97.246 ± 0.002°
• γ: 90°
• Cell volume: 5256.3 ± 1.5 ų
• Cell temperature: 296 ± 2 K
• Ambient diffraction temperature: 296 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0439
• Residual factor for significantly intense reflections: 0.0313
• Weighted residual factors for significantly intense reflections: 0.0751
• Weighted residual factors for all reflections included in the refinement: 0.0797
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No